Synthesis of ZnFe2O4 from metallic zinc and iron by wet-milling process

Sadan Ozcan; Burak Kaynar; Musa Mutlu Can; Tezer Firat

doi:10.1016/j.mseb.2005.04.006

Synthesis of ZnFe₂O₄ from metallic zinc and iron by wet-milling process

Sadan Ozcan
, Burak Kaynar
, Musa Mutlu Can
, Tezer Firat

Hacettepe University

Research output: Contribution to journal › Article › peer-review

50 Citations (Scopus)

Abstract

Nanosized zinc ferrite (ZnFe₂O₄) has been prepared directly from metallic iron (Fe) and zinc (Zn) powders by using wet-milling technique. Structural and magnetic properties of the samples were investigated by X-ray diffraction (XRD), thermo gravimetric analysis (TGA) and vibrating sample magnetometer (VSM). It is found that the particle size varied from 38.2 to 19.4 nm as the milling time was increased from 2 to 20 h. Magnetic measurements at room temperature revealed that the magnetization of the samples increased as the particle size decreased.

Original language	English
Pages (from-to)	278-281
Number of pages	4
Journal	Materials Science and Engineering: B
Volume	121
Issue number	3
DOIs	https://doi.org/10.1016/j.mseb.2005.04.006
Publication status	Published - 15 Aug 2005

Keywords

Magnetic measurements
Mechanical alloying
Nanostructure
X-ray diffraction
Zinc ferrite

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10.1016/j.mseb.2005.04.006

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title = "Synthesis of ZnFe2O4 from metallic zinc and iron by wet-milling process",

abstract = "Nanosized zinc ferrite (ZnFe2O4) has been prepared directly from metallic iron (Fe) and zinc (Zn) powders by using wet-milling technique. Structural and magnetic properties of the samples were investigated by X-ray diffraction (XRD), thermo gravimetric analysis (TGA) and vibrating sample magnetometer (VSM). It is found that the particle size varied from 38.2 to 19.4 nm as the milling time was increased from 2 to 20 h. Magnetic measurements at room temperature revealed that the magnetization of the samples increased as the particle size decreased.",

keywords = "Magnetic measurements, Mechanical alloying, Nanostructure, X-ray diffraction, Zinc ferrite",

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AU - Ozcan, Sadan

AU - Kaynar, Burak

AU - Can, Musa Mutlu

AU - Firat, Tezer

PY - 2005/8/15

Y1 - 2005/8/15

N2 - Nanosized zinc ferrite (ZnFe2O4) has been prepared directly from metallic iron (Fe) and zinc (Zn) powders by using wet-milling technique. Structural and magnetic properties of the samples were investigated by X-ray diffraction (XRD), thermo gravimetric analysis (TGA) and vibrating sample magnetometer (VSM). It is found that the particle size varied from 38.2 to 19.4 nm as the milling time was increased from 2 to 20 h. Magnetic measurements at room temperature revealed that the magnetization of the samples increased as the particle size decreased.

AB - Nanosized zinc ferrite (ZnFe2O4) has been prepared directly from metallic iron (Fe) and zinc (Zn) powders by using wet-milling technique. Structural and magnetic properties of the samples were investigated by X-ray diffraction (XRD), thermo gravimetric analysis (TGA) and vibrating sample magnetometer (VSM). It is found that the particle size varied from 38.2 to 19.4 nm as the milling time was increased from 2 to 20 h. Magnetic measurements at room temperature revealed that the magnetization of the samples increased as the particle size decreased.

KW - Magnetic measurements

KW - Mechanical alloying

KW - Nanostructure

KW - X-ray diffraction

KW - Zinc ferrite

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JO - Materials Science and Engineering: B

JF - Materials Science and Engineering: B

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ER -

Synthesis of ZnFe₂O₄ from metallic zinc and iron by wet-milling process

Abstract

Keywords

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