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Identification by HPLC-PAD-MS and quantification by HPLC-PAD of phenylethanoid glycosides of five Phlomis species

  • Hasan Kirmizibekmez
  • , Paola Montoro
  • , Sonia Piacente
  • , Cosimo Pizza
  • , Ali Dönmez
  • , Ihsan Çaliş
  • Hacettepe University
  • University of Salerno

Research output: Contribution to journalArticlepeer-review

79 Citations (Scopus)

Abstract

The qualitative and quantitative determination of phenylethanoid glycosides in methanolic extracts of five species of the genus Phlomis (Lamiaceae) has been investigated using a new reversed-phase HPLC method combined with photodiode-array detection and electrospray/MS analysis. Forsythoside B, verbascoside, samioside, alyssonoside, isoverbascoside, leucosceptosides A and B and martynoside were detected. The quantification of the above constituents was performed using echinacoside as internal standard. Knowledge of the content of phenylethanoid glycosides contributes to the chemotaxonomy of the genus.

Original languageEnglish
Pages (from-to)1-6
Number of pages6
JournalPhytochemical Analysis
Volume16
Issue number1
DOIs
Publication statusPublished - 2005

Keywords

  • ESI/MS
  • HPLC-MS
  • HPLC-PAD
  • Phenylethanoid glycosides
  • Phlomis bruguieri
  • Phlomis kurdica
  • Phlomis leucophractha
  • Phlomis nissolii
  • Phlomis russeliana

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