Dimethyl 6-bromo-2-methyl-1,2-dihydroquinoline-2,4-dicarboxylate

Zeynep Gültekin; Michael Bolte; Tuncer Hökelek

doi:10.1107/S1600536812005600

Dimethyl 6-bromo-2-methyl-1,2-dihydroquinoline-2,4-dicarboxylate

Zeynep Gültekin
, Michael Bolte
, Tuncer Hökelek

Hacettepe University

Çankr Karatekin University
Goethe University Frankfurt

Research output: Contribution to journal › Article › peer-review

2 Citations (Scopus)

Abstract

In the title compound, C ₁₄H ₁₄BrNO ₄, the dihydro-pyridine ring adopts a screw-boat conformation. In the crystal, pairs of N - H⋯O hydrogen bonds link the molecules into inversion R ₂ ²(10) dimers.

Original language	English
Pages (from-to)	o710-o711
Journal	Acta Crystallographica Section E: Structure Reports Online
Volume	68
Issue number	3
DOIs	https://doi.org/10.1107/S1600536812005600
Publication status	Published - Mar 2012

Keywords

R factor = 0.053
T = 173 K
data-to-parameter ratio = 14.2
mean σ(C-C) = 0.007 Å
single-crystal X-ray study
wR factor = 0.153

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@article{dae9253a5547429db9b858fe88457665,

title = "Dimethyl 6-bromo-2-methyl-1,2-dihydroquinoline-2,4-dicarboxylate",

abstract = "In the title compound, C 14H 14BrNO 4, the dihydro-pyridine ring adopts a screw-boat conformation. In the crystal, pairs of N - H⋯O hydrogen bonds link the molecules into inversion R 2 2(10) dimers.",

keywords = "R factor = 0.053, T = 173 K, data-to-parameter ratio = 14.2, mean σ(C-C) = 0.007 {\AA}, single-crystal X-ray study, wR factor = 0.153",

author = "Zeynep G{\"u}ltekin and Michael Bolte and Tuncer H{\"o}kelek",

year = "2012",

month = mar,

doi = "10.1107/S1600536812005600",

language = "English",

volume = "68",

pages = "o710--o711",

journal = "Acta Crystallographica Section E: Structure Reports Online",

issn = "1600-5368",

publisher = "International Union of Crystallography",

number = "3",

}

TY - JOUR

T1 - Dimethyl 6-bromo-2-methyl-1,2-dihydroquinoline-2,4-dicarboxylate

AU - Gültekin, Zeynep

AU - Bolte, Michael

AU - Hökelek, Tuncer

PY - 2012/3

Y1 - 2012/3

N2 - In the title compound, C 14H 14BrNO 4, the dihydro-pyridine ring adopts a screw-boat conformation. In the crystal, pairs of N - H⋯O hydrogen bonds link the molecules into inversion R 2 2(10) dimers.

AB - In the title compound, C 14H 14BrNO 4, the dihydro-pyridine ring adopts a screw-boat conformation. In the crystal, pairs of N - H⋯O hydrogen bonds link the molecules into inversion R 2 2(10) dimers.

KW - R factor = 0.053

KW - T = 173 K

KW - data-to-parameter ratio = 14.2

KW - mean σ(C-C) = 0.007 Å

KW - single-crystal X-ray study

KW - wR factor = 0.153

UR - https://www.scopus.com/pages/publications/84857927292

U2 - 10.1107/S1600536812005600

DO - 10.1107/S1600536812005600

M3 - Article

AN - SCOPUS:84857927292

SN - 1600-5368

VL - 68

SP - o710-o711

JO - Acta Crystallographica Section E: Structure Reports Online

JF - Acta Crystallographica Section E: Structure Reports Online

IS - 3

ER -

Dimethyl 6-bromo-2-methyl-1,2-dihydroquinoline-2,4-dicarboxylate

Abstract

Keywords

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