Crystal structure of 3,4:11,12-Dibenzo-5,10-dioxa-1,14,17-tri-azacyclononadecane

Tuncer Hökelek; Elif Ece Ilter; Nuran Asmafiliz; Zeynel Kiliç

doi:10.2116/analscix.20.x163

Crystal structure of 3,4:11,12-Dibenzo-5,10-dioxa-1,14,17-tri-azacyclononadecane

Tuncer Hökelek
, Elif Ece Ilter
, Nuran Asmafiliz
, Zeynel Kiliç

Hacettepe University

Ankara University

Research output: Contribution to journal › Comment/debate

Abstract

The title compound, C₂₂H₃₁N₃O₂, consists of a 19-membered triaza-crown ether ligand with two O atoms and three N atoms. It belongs to the space group C2/c with cell parameters a = 26.753(3), b = 9.1004(18), c = 19.160(3)Å and β = 115.950(12)°. The macrocyclic ring contains N-H·O hydrogen bonds. The relative macrocyclic inner-hole size is estimated to be 1.93 Å. 2004

Original language	English
Pages (from-to)	x163-x164
Journal	Analytical Sciences: X-ray Structure Analysis Online
Volume	20
Issue number	4
DOIs	https://doi.org/10.2116/analscix.20.x163
Publication status	Published - 2004

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@article{c1306100bd464923bb86b21297b30c06,

title = "Crystal structure of 3,4:11,12-Dibenzo-5,10-dioxa-1,14,17-tri-azacyclononadecane",

abstract = "The title compound, C22H31N3O2, consists of a 19-membered triaza-crown ether ligand with two O atoms and three N atoms. It belongs to the space group C2/c with cell parameters a = 26.753(3), b = 9.1004(18), c = 19.160(3){\AA} and β = 115.950(12)°. The macrocyclic ring contains N-H·O hydrogen bonds. The relative macrocyclic inner-hole size is estimated to be 1.93 {\AA}. 2004",

author = "Tuncer H{\"o}kelek and Ilter, \{Elif Ece\} and Nuran Asmafiliz and Zeynel Kili{\c c}",

year = "2004",

doi = "10.2116/analscix.20.x163",

language = "English",

volume = "20",

pages = "x163--x164",

journal = "Analytical Sciences: X-ray Structure Analysis Online",

issn = "1348-2238",

publisher = "Japan Society for Analytical Chemistry",

number = "4",

}

TY - JOUR

T1 - Crystal structure of 3,4:11,12-Dibenzo-5,10-dioxa-1,14,17-tri-azacyclononadecane

AU - Hökelek, Tuncer

AU - Ilter, Elif Ece

AU - Asmafiliz, Nuran

AU - Kiliç, Zeynel

PY - 2004

Y1 - 2004

N2 - The title compound, C22H31N3O2, consists of a 19-membered triaza-crown ether ligand with two O atoms and three N atoms. It belongs to the space group C2/c with cell parameters a = 26.753(3), b = 9.1004(18), c = 19.160(3)Å and β = 115.950(12)°. The macrocyclic ring contains N-H·O hydrogen bonds. The relative macrocyclic inner-hole size is estimated to be 1.93 Å. 2004

AB - The title compound, C22H31N3O2, consists of a 19-membered triaza-crown ether ligand with two O atoms and three N atoms. It belongs to the space group C2/c with cell parameters a = 26.753(3), b = 9.1004(18), c = 19.160(3)Å and β = 115.950(12)°. The macrocyclic ring contains N-H·O hydrogen bonds. The relative macrocyclic inner-hole size is estimated to be 1.93 Å. 2004

UR - https://www.scopus.com/pages/publications/70450233838

U2 - 10.2116/analscix.20.x163

DO - 10.2116/analscix.20.x163

M3 - Comment/debate

AN - SCOPUS:70450233838

SN - 1348-2238

VL - 20

SP - x163-x164

JO - Analytical Sciences: X-ray Structure Analysis Online

JF - Analytical Sciences: X-ray Structure Analysis Online

IS - 4

ER -

Crystal structure of 3,4:11,12-Dibenzo-5,10-dioxa-1,14,17-tri-azacyclononadecane

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