6,6-[Ethyl-enebis(sulfanediyl)]-2-(2-methoxy-ethyl)-1,2,3,4,5, 6-hexa-hydro-1,5-methano-1H-azocino[4,3-b]indol-3-one

Baris Tercan; Fatma Yüksel; Süleyman Patr; Tuncer Hökelek

doi:10.1107/S1600536810015941

6,6-[Ethyl-enebis(sulfanediyl)]-2-(2-methoxy-ethyl)-1,2,3,4,5, 6-hexa-hydro-1,5-methano-1H-azocino[4,3-b]indol-3-one

Baris Tercan
, Fatma Yüksel
, Süleyman Patr
, Tuncer Hökelek

Hacettepe University

Karabuk University
Gebze Technical University
Hacettepe University

Research output: Contribution to journal › Article › peer-review

5 Citations (Scopus)

Abstract

The title compound, C₁₉H₂₂N₂O ₂S₂, consists of a tetra-cyclic ring system containing an azocine skeleton with methoxy-ethyl and dithiol-ane groups as substituents. The benzene and five-membered N-heterocyclic rings are nearly coplanar, making a dihedral angle of 0.81 (12)°. The dithiol-ane ring adopts an envelope conformation. Inter-molecular N - H⋯O hydrogen-bonding and weak C - H⋯π inter-actions are present in the crystal structure.

Original language	English
Pages (from-to)	o1275-o1276
Journal	Acta Crystallographica Section E: Structure Reports Online
Volume	66
Issue number	6
DOIs	https://doi.org/10.1107/S1600536810015941
Publication status	Published - 2010

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title = "6,6-[Ethyl-enebis(sulfanediyl)]-2-(2-methoxy-ethyl)-1,2,3,4,5, 6-hexa-hydro-1,5-methano-1H-azocino[4,3-b]indol-3-one",

abstract = "The title compound, C19H22N2O 2S2, consists of a tetra-cyclic ring system containing an azocine skeleton with methoxy-ethyl and dithiol-ane groups as substituents. The benzene and five-membered N-heterocyclic rings are nearly coplanar, making a dihedral angle of 0.81 (12)°. The dithiol-ane ring adopts an envelope conformation. Inter-molecular N - H⋯O hydrogen-bonding and weak C - H⋯π inter-actions are present in the crystal structure.",

author = "Baris Tercan and Fatma Y{\"u}ksel and S{\"u}leyman Patr and Tuncer H{\"o}kelek",

year = "2010",

doi = "10.1107/S1600536810015941",

language = "English",

volume = "66",

pages = "o1275--o1276",

journal = "Acta Crystallographica Section E: Structure Reports Online",

issn = "1600-5368",

publisher = "International Union of Crystallography",

number = "6",

}

TY - JOUR

T1 - 6,6-[Ethyl-enebis(sulfanediyl)]-2-(2-methoxy-ethyl)-1,2,3,4,5, 6-hexa-hydro-1,5-methano-1H-azocino[4,3-b]indol-3-one

AU - Tercan, Baris

AU - Yüksel, Fatma

AU - Patr, Süleyman

AU - Hökelek, Tuncer

PY - 2010

Y1 - 2010

N2 - The title compound, C19H22N2O 2S2, consists of a tetra-cyclic ring system containing an azocine skeleton with methoxy-ethyl and dithiol-ane groups as substituents. The benzene and five-membered N-heterocyclic rings are nearly coplanar, making a dihedral angle of 0.81 (12)°. The dithiol-ane ring adopts an envelope conformation. Inter-molecular N - H⋯O hydrogen-bonding and weak C - H⋯π inter-actions are present in the crystal structure.

AB - The title compound, C19H22N2O 2S2, consists of a tetra-cyclic ring system containing an azocine skeleton with methoxy-ethyl and dithiol-ane groups as substituents. The benzene and five-membered N-heterocyclic rings are nearly coplanar, making a dihedral angle of 0.81 (12)°. The dithiol-ane ring adopts an envelope conformation. Inter-molecular N - H⋯O hydrogen-bonding and weak C - H⋯π inter-actions are present in the crystal structure.

UR - https://www.scopus.com/pages/publications/77953222772

U2 - 10.1107/S1600536810015941

DO - 10.1107/S1600536810015941

M3 - Article

AN - SCOPUS:77953222772

SN - 1600-5368

VL - 66

SP - o1275-o1276

JO - Acta Crystallographica Section E: Structure Reports Online

JF - Acta Crystallographica Section E: Structure Reports Online

IS - 6

ER -

6,6-[Ethyl-enebis(sulfanediyl)]-2-(2-methoxy-ethyl)-1,2,3,4,5, 6-hexa-hydro-1,5-methano-1H-azocino[4,3-b]indol-3-one

Abstract

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