4-(Furan-2-ylmethoxy)benzene-1,2-dicarbonitrile

Hülya Tuncer; Ahmet Orhan Görgülü; Tuncer Hökelek

doi:10.1107/S1600536811053669

4-(Furan-2-ylmethoxy)benzene-1,2-dicarbonitrile

Hülya Tuncer
, Ahmet Orhan Görgülü
, Tuncer Hökelek

Hacettepe University

Firat University

Research output: Contribution to journal › Article › peer-review

4 Citations (Scopus)

Abstract

In the title compound, C ₁₃H ₈N ₂O ₂, prepared from furfuryl alcohol and 4-nitrophthalonitrile in the presence of potassium carbonate in dimethylformamide, the furan and benzene rings are oriented at a dihedral angle of 53.45(9)°. In the crystal, weak C-H···O and C-H···N hydrogen bonds link the molecules into a three-dimensional network.

Original language	English
Pages (from-to)	o153
Journal	Acta Crystallographica Section E: Structure Reports Online
Volume	68
Issue number	1
DOIs	https://doi.org/10.1107/S1600536811053669
Publication status	Published - Jan 2012

Keywords

Data-to-parameter ratio = 17.0
Mean σ(C-C) = 0.004 Å
R factor = 0.048
Single-crystal X-ray study
T = 100 K
wR factor = 0.141

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title = "4-(Furan-2-ylmethoxy)benzene-1,2-dicarbonitrile",

abstract = "In the title compound, C 13H 8N 2O 2, prepared from furfuryl alcohol and 4-nitrophthalonitrile in the presence of potassium carbonate in dimethylformamide, the furan and benzene rings are oriented at a dihedral angle of 53.45(9)°. In the crystal, weak C-H···O and C-H···N hydrogen bonds link the molecules into a three-dimensional network.",

keywords = "Data-to-parameter ratio = 17.0, Mean σ(C-C) = 0.004 {\AA}, R factor = 0.048, Single-crystal X-ray study, T = 100 K, wR factor = 0.141",

author = "H{\"u}lya Tuncer and G{\"o}rg{\"u}l{\"u}, \{Ahmet Orhan\} and Tuncer H{\"o}kelek",

year = "2012",

month = jan,

doi = "10.1107/S1600536811053669",

language = "English",

volume = "68",

pages = "o153",

journal = "Acta Crystallographica Section E: Structure Reports Online",

issn = "1600-5368",

publisher = "International Union of Crystallography",

number = "1",

}

TY - JOUR

T1 - 4-(Furan-2-ylmethoxy)benzene-1,2-dicarbonitrile

AU - Tuncer, Hülya

AU - Görgülü, Ahmet Orhan

AU - Hökelek, Tuncer

PY - 2012/1

Y1 - 2012/1

N2 - In the title compound, C 13H 8N 2O 2, prepared from furfuryl alcohol and 4-nitrophthalonitrile in the presence of potassium carbonate in dimethylformamide, the furan and benzene rings are oriented at a dihedral angle of 53.45(9)°. In the crystal, weak C-H···O and C-H···N hydrogen bonds link the molecules into a three-dimensional network.

AB - In the title compound, C 13H 8N 2O 2, prepared from furfuryl alcohol and 4-nitrophthalonitrile in the presence of potassium carbonate in dimethylformamide, the furan and benzene rings are oriented at a dihedral angle of 53.45(9)°. In the crystal, weak C-H···O and C-H···N hydrogen bonds link the molecules into a three-dimensional network.

KW - Data-to-parameter ratio = 17.0

KW - Mean σ(C-C) = 0.004 Å

KW - R factor = 0.048

KW - Single-crystal X-ray study

KW - T = 100 K

KW - wR factor = 0.141

UR - https://www.scopus.com/pages/publications/84855365274

U2 - 10.1107/S1600536811053669

DO - 10.1107/S1600536811053669

M3 - Article

C2 - 22259439

AN - SCOPUS:84855365274

SN - 1600-5368

VL - 68

SP - o153

JO - Acta Crystallographica Section E: Structure Reports Online

JF - Acta Crystallographica Section E: Structure Reports Online

IS - 1

ER -

4-(Furan-2-ylmethoxy)benzene-1,2-dicarbonitrile

Abstract

Keywords

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